A new analytical approach for preconcentration, separation and determination of Pb(II) and Cd(II) in real samples using a new adsorbent: Synthesis, characterization and application

Basit Öğe Kaydı
dc.authorid0000-0001-8770-805X
dc.contributor.authorAltunay, Nail
dc.contributor.authorHazer, Baki
dc.contributor.authorTüzen, Mustafa
dc.contributor.authorElik, Adil
dc.date.accessioned2021-08-19T06:30:00Z
dc.date.available2021-08-19T06:30:00Z
dc.date.issued2021en_US
dc.departmentKapadokya Üniversitesi, Uygulamalı Bilimler Yüksekokulu, Uçak Gövde ve Motor Bakımı Bölümü
dc.descriptionTARAMAWOS
dc.descriptionTARAMAPUBMED
dc.descriptionTARAMASCOPUS
dc.description.abstractA green and efficient analytical approach was reported for simultaneous preconcentration, and separation of Pb (II) and Cd(II) in water, vegetables, and barbecue samples by dispersive solid-phase microextraction prior to their determination using flame atomic absorption spectrometry. A new poly-3-hydroxy butyrate-polyvinyl triethyl ammonium chloride comb-type amphiphilic cationic block copolymer (PHBvbNCl) was synthesized and char acterized. Main variables such as pH, sorbent amount, adsorption time, eluent type, desorption time, and sample volume were optimized. Detection limits and working ranges for Pb(II) and Cd(II) were 0.03 ?g L-1, 0.15 ?g L-1, 0.1–250 ?g L-1 and 0.5–375 ?g L-1, respectively. Enhancement factor for Pb (II) and Cd (II) were 114 and 98. The adsorption capacity of PHBvbNCl for Pb(II) and Cd(II) was 175.2 mg g? 1 and 152.9 mg g? 1 . After the accuracy of the method was confirmed by the analysis of certified reference materials, it was successfully applied to real samples. Finally, the analytical performance of the present method was compared with other methods.
dc.identifier.citationALTUNAY, N., HAZER, B., TÜZEN, M., & ELİK, A. (2021). A new analytical approach for preconcentration separation and determination of Pb II and Cd II in real samples using a new adsorbent Synthesis characterization and application. Food Chemistry, 359, 0–0.
dc.identifier.doi10.1016/j.foodchem.2021.129923
dc.identifier.endpage8en_US
dc.identifier.scopusqualityQ1
dc.identifier.startpage1en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12695/1252
dc.identifier.volume359en_US
dc.identifier.wosWOS:000663770100005
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Sceince
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorHazer, Baki
dc.language.isoen
dc.publisherElseiver
dc.relation.ispartofFood Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectLead
dc.subjectCadmium
dc.subjectSolid phase microextraction
dc.subjectCationic polymer sorbent
dc.subjectVegetables and barbecue samples
dc.titleA new analytical approach for preconcentration, separation and determination of Pb(II) and Cd(II) in real samples using a new adsorbent: Synthesis, characterization and application
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
A new analytical approach for preconcentration.pdf
Boyut:
2.24 MB
Biçim:
Adobe Portable Document Format
Açıklama:
Makale / Article
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Uçak Gövde ve Motor Bakımı - Makale Koleksiyonu