Development of sensitive and accurate solid-phase microextraction procedure for preconcentration of As(III) ions in real samples

Basit Öğe Kaydı
dc.authorid0000-0001-8770-805X
dc.contributor.authorElik, Adil
dc.contributor.authorTüzen, Mustafa
dc.contributor.authorHazer, Baki
dc.contributor.authorKaya, Savaş
dc.contributor.authorKatin, K.P
dc.contributor.authorAltunay, Nail
dc.date.accessioned2021-08-19T06:40:25Z
dc.date.available2021-08-19T06:40:25Z
dc.date.issued2021en_US
dc.departmentKapadokya Üniversitesi, Uygulamalı Bilimler Yüksekokulu, Uçak Gövde ve Motor Bakımı Bölümü
dc.descriptionTARAMAWOS
dc.descriptionTARAMAPUBMED
dc.descriptionTARAMASCOPUS
dc.description.abstractWe synthesized the poly(methyl methacrylate-co-2-aminoethyl methacrylate (PMaema) amphiphilic copolymer in a form of solid phase adsorbent. Then it was used for separation, preconcentration and determination of trace amount of As(III) ions from foods and waters with hydride generation atomic absorption spectrometry. The PMaema was characterized by fourier transform infrared spectrometer and nuclear magnetic resonance spectrometer. The adsorption of As(III) to the PMaema was also supported using computational chemistry studies. The experimental parameters (pH, PMaema amount, adsorption time and ethanol volume) were optimized using a three-level Box–Behnken design with four experimental factors. We observed linear calibration curve for the PMaema amount in the 10–500 ng L?1 range (R2 = 0.9956). Limit of detection, preconcentration factor and sorbent capacity of PMaema were equal to 3.3 ng L?1, 100 and 75.8 mg ­g?1, respectively. The average recoveries (spiked at 50 ng ­L?1) changes in the range of 91.5–98.6% with acceptable relative standard deviation less than 4.3%. After validation studies, the method was successfully applied for separation, preconcentration and determination of trace amount of As(III) from foods and waters.
dc.identifier.citationHAZER, B., ELİK, A., TÜZEN, M., KAYA, S., ALTUNAY, N., & Katin, K. . (2021). Development of sensitive and accurate solid-phase microextraction procedure for preconcentration of As III ions in real samples. Scientific Reports, 11, 0–0.
dc.identifier.doi10.1038/s41598-021-84819-0
dc.identifier.endpage16en_US
dc.identifier.scopusqualityQ1
dc.identifier.startpage1en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12695/1254
dc.identifier.wosWOS:000630437600011
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Sceince
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorHazer, Baki
dc.language.isoen
dc.relation.ispartofScientific Reports
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subject[Keywords Not Available]
dc.titleDevelopment of sensitive and accurate solid-phase microextraction procedure for preconcentration of As(III) ions in real samples
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Küçük Resim
İsim:
Development of sensitive.pdf
Boyut:
4.55 MB
Biçim:
Adobe Portable Document Format
Açıklama:
Makale / Article
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

UGM - Makale Koleksiyonu