Poly(styrene)-co-2-vinylpyridine copolymer as a novel solid-phase adsorbent for determination of manganese and zinc in foods and vegetables by FAAS

Basit Öğe Kaydı
dc.authorid0000-0001-8770-805X
dc.contributor.authorTüzen, Mustafa
dc.contributor.authorElik, Adil
dc.contributor.authorHazer, Baki
dc.contributor.authorŞimşek, Selçuk
dc.contributor.authorAltunay, Nail
dc.date.accessioned2021-08-19T06:46:26Z
dc.date.available2021-08-19T06:46:26Z
dc.date.issued2020en_US
dc.departmentKapadokya Üniversitesi, Uygulamalı Bilimler Yüksekokulu, Uçak Gövde ve Motor Bakımı Bölümü
dc.descriptionTARAMAPUBMED
dc.descriptionTARAMASCOPUS
dc.description.abstracthe aim of this study is to extract zinc and manganese from foods and vegetables using an amphiphilic copo lymer adsorbent, poly(styrene)-co-2-vinylpyridine which was synthesized via reversible addition fragmentation chain transfer (RAFT) polymerization from styrene and 2-vinyl pyridine in the presence of a trithiocarbonate and 2,2?-azo-bis isobutyro nitrile (AIBN) in toluene solution under argon at 80 °C. Fourier Transform Infrared (FTIR) and proton nuclear magnetic resonance (1 H NMR) spectroscopy were used in the characterization of the ob tained copolymer. Under the optimum conditions, several validation variables such as uncertainty measurement, selectivity, robustness, precisions, matrix effects and accuracy were investigated. Taking an adsorption time of 15 min, detection limits of 0.04 ?g L ?1 and 0.2 ?g L ?1 and 7.9 ?g L?1 and enrichment factors of 145 and 110 were obtained for Mn(II) and Zn(II), respectively. The method was successfully applied to the analysis of Mn(II) and Zn(II) in foods and vegetables.
dc.identifier.citationHAZER, B., TÜZEN, M., ELİK, A., ŞİMŞEK, S., & ALTUNAY, N. (2020). Poly styrene -co-2-vinylpyridine copolymer as a novel solid-phase adsorbent for determination of manganese and zinc in foods and vegetables by FAAS. Food Chemistry, 333, 0–0.
dc.identifier.doi10.1016/j.foodchem.2020.127504
dc.identifier.endpage9en_US
dc.identifier.issue333en_US
dc.identifier.scopusqualityQ1
dc.identifier.startpage1en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12695/1256
dc.identifier.wosWOS:000606843000008
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Sceince
dc.indekslendigikaynakScopus
dc.indekslendigikaynakPubMed
dc.institutionauthorHazer, Baki
dc.language.isoen
dc.publisherElseiver
dc.relation.ispartofFood Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectZinc
dc.subjectManganese
dc.subjectFood
dc.subjectVegetable
dc.subjectAmphiphilic copolymer
dc.subjectSolid-phase microextraction
dc.titlePoly(styrene)-co-2-vinylpyridine copolymer as a novel solid-phase adsorbent for determination of manganese and zinc in foods and vegetables by FAAS
dc.typeArticle

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